Tri-p-tolyl­phosphine

نویسندگان

  • Hao Wang
  • Yi-Bin Wang
  • Bo-Nian Liu
  • Shi-Gui Tang
  • Ping Wei
چکیده

In the title compound C(21)H(21)P, the P atom is situated on a crystallographic threefold rotatory-inversion axis, resulting in threefold rotation symmetry of the title compound. The dihedral angles between the symmetry-related benzene rings are 87.40 (18)°.

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The title compound, [RhCl(C(21)H(21)P)(2)(CO)]·C(3)H(6)O, was precipitated in trace yield from a reaction of RhCl(cod)(THP) with P(p-tol)(3) in a 1:1 acetone-d(6)/CD(3)OD solution under a hydrogen atmosphere [p-tol = p-tolyl, THP = tris-(hydroxy-meth-yl)phosphine, P(CH(2)OH)(3), and cod = 1,5-cyclo-octa-diene]. The complex displays a square-planar geometry around the Rh(I) atom. The complex mol...

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عنوان ژورنال:

دوره 64  شماره 

صفحات  -

تاریخ انتشار 2008